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发帖数: 50 | 1 I want to polymerize poly(ethylene glycol) and lactide in 150 degree, stannous
octoate as catalyst. no water and high vacuum is very important.
In fact, many papers have described the polymerization: a polymerization tube
or flask connected with vacuum pump.
However, i found it's very difficult to find a suitable flask and very
difficult to keep the vacuum during the reaction.
Anyone who do this can teach me?
Thanks a lot!! |
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